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the precipitated silica using no. whatman filter paper or equivalent and wash with hot % by vol hydrochloric acid. finally wash with hot water. scrub the beaker to remove any adhering silica. transfer the clear filtrate to the original beaker and repeat the dehydration directly on the hot plate. exercise

care to avoid splattering as the volume decreases. bake the residue carefully to remove all acid and continue baking on an asbestos pad for hr to dehydrate completely the last traces of silica. cool, dissolve salt as previously indicated, and filter on no. whatman paper or equivalent. wash as previously...

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